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Hydrogen-Induced Cracking (HIC / SOHIC) – NACE TM0284 / TM0103

Standard method to assess the resistance of pipelines, pressure vessels, and steel plates to hydrogen-induced cracking in H₂S environments; optical evaluation yields crack sensitivity, crack length, and crack thickness ratios to judge susceptibility and ensure durability.

Overview

Detect hydrogen-induced cracking in H₂S service

HIC occurs when atomic hydrogen, absorbed via aqueous sulfide corrosion, diffuses into carbon or low-alloy steels and forms molecular hydrogen that builds internal pressure and initiates cracks. The NACE TM0284 / TM0103 method evaluates resistance by calculating crack sensitivity, crack length, and crack thickness ratios from optical examination of test pieces—supporting durability and safety in H₂S-rich environments.

ISO/IEC 17025:2017 accredited practices and reporting.
Media

Test solutions

A

NaCl + acetic acid

A solution of sodium chloride and acetic acid (NaCl, CH₃COOH) saturated with H₂S at temperature and ambient pressure.

B

Synthetic seawater

A solution of synthetic seawater saturated with H₂S at ambient temperature and pressure.

Setup

Reagents

  • Inert gas for purging.
  • Mixture of H₂S and CO₂ with H₂S content sufficient to produce the specified H₂S partial pressure.
  • NaCl and CH₃COONa.
  • HCl or NaOH to achieve the specified pH.
  • Distilled or deionized water.
Benefits

Why this test matters

Material suitability

Identifies susceptibility to HIC / SOHIC for components in H₂S-rich environments.

Safety & durability

Supports prevention of failures in pipelines, pressure vessels, and structural plates.

Get in touch

Talk to an expert

Send alloy grade, thickness, and target environment. We’ll confirm the HIC/SOHIC plan, endpoints, and reporting.

ISO/IEC 17025:2017 accredited