Oxalic Acid Test
Rapid screening by oxalic acid etching.
Critical testing guidelines for qualifying stainless-steel products against intergranular corrosion (IGC) to meet industry performance requirements.
Intergranular corrosion testing evaluates deterioration at grain boundaries—often due to carbide precipitation—so you can qualify material batches and confirm heat-treatment effectiveness across stainless-steel families.
Applicable to austenitic grades; used for rapid screening of batches for susceptibility to IGC. The practice contains five unique tests.
Rapid screening by oxalic acid etching.
Corrosion test per practice B.
Multi-boil nitric acid exposure.
Bend/exposure per practice E.
Alternate medium with copper sulphate.
Detects susceptibility to intergranular attack in ferritic stainless steels; includes oxalic acid etch, ferritic sulfuric acid, copper sulphate–50% sulfuric acid, and copper sulfate–16% sulfuric acid tests, with microscopic examination (≈40×) and bend evaluations where specified.
Structure/attack indication via etching.
Immersion test; microscopic exam ~40×.
Copper sulphate + sulfuric acid procedure.
Alternate concentration test; exam & bends.
Used to detect the presence of intermetallic phases in duplex stainless steels that can significantly affect corrosion resistance; supports verification of heat-treatment effectiveness.
Screen batches and verify processing windows across stainless-steel families.
Demonstrate compliance with industry requirements before deployment.
Clear acceptance criteria, micrographs, and decisions for QA/QC.
Send grade (Austenitic/Ferritic/Duplex), prior heat-treatment, and target practice. We’ll confirm specimen prep, exposure, and acceptance criteria.