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Intergranular Corrosion Testing – Austenitic, Ferritic & Duplex Stainless Steels

Critical testing guidelines for qualifying stainless-steel products against intergranular corrosion (IGC) to meet industry performance requirements.

Overview

Detect susceptibility to IGC from processing or composition

Intergranular corrosion testing evaluates deterioration at grain boundaries—often due to carbide precipitation—so you can qualify material batches and confirm heat-treatment effectiveness across stainless-steel families.

ISO/IEC 17025:2017 accredited practices and reporting.
Austenitic stainless steels

ASTM A262 – Five intergranular corrosion methods

Applicable to austenitic grades; used for rapid screening of batches for susceptibility to IGC. The practice contains five unique tests.

A

Oxalic Acid Test

Rapid screening by oxalic acid etching.

B

Streicher Test

Corrosion test per practice B.

C

Huey Test

Multi-boil nitric acid exposure.

E

Strauss Test

Bend/exposure per practice E.

F

Copper Sulphate Test

Alternate medium with copper sulphate.

Ferritic stainless steels

ASTM A763 – Practices W, X, Y, Z

Detects susceptibility to intergranular attack in ferritic stainless steels; includes oxalic acid etch, ferritic sulfuric acid, copper sulphate–50% sulfuric acid, and copper sulfate–16% sulfuric acid tests, with microscopic examination (≈40×) and bend evaluations where specified.

W

Oxalic acid etch

Structure/attack indication via etching.

X

Ferritic sulfuric acid

Immersion test; microscopic exam ~40×.

Y

CuSO₄ – 50% H₂SO₄

Copper sulphate + sulfuric acid procedure.

Z

CuSO₄ – 16% H₂SO₄

Alternate concentration test; exam & bends.

“Test methods for qualifying ferritic stainless-steel products by detecting susceptibility to intergranular corrosion (IGC).”
Duplex stainless steels

ASTM A923 – Intermetallic phases & heat treatment

Used to detect the presence of intermetallic phases in duplex stainless steels that can significantly affect corrosion resistance; supports verification of heat-treatment effectiveness.

Benefits

Why this testing matters

Material qualification

Screen batches and verify processing windows across stainless-steel families.

Performance assurance

Demonstrate compliance with industry requirements before deployment.

Actionable reporting

Clear acceptance criteria, micrographs, and decisions for QA/QC.

Get in touch

Talk to an expert

Send grade (Austenitic/Ferritic/Duplex), prior heat-treatment, and target practice. We’ll confirm specimen prep, exposure, and acceptance criteria.

ISO/IEC 17025:2017 Accredited · www.mett-bio.com